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The sample had no residual carbon no peak at 272 eV and oxygen no peak at 510 eV both after ultra-high vacuum cleaning the silicon surface and after the growth of the calcium silicide film Fig. 1 a , when an intense Ca peak appeared 301 eV on the AES spectrum. The actual concentration of impurity atoms can be estimated at less than 0.1% ...

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A method and apparatus for treating a bath of liquid iron or steel by submerged injection of a gas or gas-entrained particulate re-agents. Injection is through a tuyere occludable either by a stopper rod assembly or by a sliding gate valve and the bath treatment may include desulphurizing, deoxidizing, alloying or sulphide modifying.

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